Malaysian Journal of Analytical Sciences Vol 18 No 2 (2014): 434 -
443
MECHANICAL PROPERTIES OF STARCH FILLED
POLYPROPYLENE UNDER EXPOSURE OF HYGROTHERMAL CONDITIONS
(Sifat-sifat
Mekanikal Bagi Komposit Polipropilena Terisi Kanji di Bawah Pendedahan Higroterma)
Wan Zakaria Wan Nor*, Nor Azura
Abdul Rahim, Hakimah Osman and Muthmirah Ibrahim
School of
Materials Engineering,
Universiti
Malaysia Perlis, Kompleks Pengajian Jejawi, Jejawi 2, 02600 Arau, Perlis,
Malaysia.
*Corresponding
author: wanzakariawannor@gmail.com
Abstract
The
hygrothermal properties of starch filled polypropylene (PP) composites with
different types of starches; sago, tapioca, and corn content at 20 wt% were
studied. The PP composites were compounded using Brabender Plasticoder machine
and the composites samples were prepared through by compression molding
technique. The hygrothermal absorption test was conducted out to investigate
the moisture absorption at different temperatures (i.e. room temperature, 40°C
and 70°C). Thus, the flexural test was carried out to study the effect of
hygrothermal conditions on mechanical properties and scanning electron
microscopy (SEM) used to verify the obtained results through morphological
study. The results revealed that the mechanical properties of PP composites
deteriorate after a period of immersion time and the hygrothermal aging of
composites was accelerated as the temperature increased.
Keywords: polypropylene
composites, starch filled polypropylene, hygrothermal absorption, mechanical properties
Abstrak
Sifat-sifat
higroterma bagi komposit polipropilena (PP) terisi kanji; sagu, ubi kayu, dan
jagung yang terkandung 20% berat telah dikaji. Komposit-komposit PP telah
disebatikan menggunakan mesin Brabender Plasticoder dan sampel-sampel komposit
disediakan menggunakan teknik pengacuanan mampatan. Ujian penyerapan higroterma
telah dijalankan untuk menyiasat kadar serapan lembapan pada beberapa suhu yang
berbeza (suhu bilik, 40°C, dan 70°C). Seterusnya, ujian lenturan telah
dijalankan untuk menkaji kesan keadaan higroterma ke atas sifat-sifat mekanikal
dan mikroskopi pengimbasan electron (SEM) digunakan untuk mengesahkan keputusan
yang diperolehi melalui kajian morfologi. Keputusan menunjukkan bahawa
sifat-sifat mekanikal bagi komposit-komposit PP merosot selepas direndam untuk
suatu tempoh masa dan kadar penuaan higroterma bagi komposit-komposit telah
dipercepatkan apabila suhu meningkat.
Kata kunci: komposit
polipropilena, polipropilena terisi kanji, serapan higroterma, sifat-sifat
mekanikal
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